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Single-crystal X-ray analysis

eagle-i ID

http://hunter-cuny.eagle-i.net/i/00000136-a7a4-c4b9-949b-425080000000

Resource Type

  1. Material analysis service

Properties

  1. Fee for service
    Yes
  2. Resource Description
    "Rules of Operation 1. The sample is examined under the microscope to see if it is suitable for single-crystal X-ray analysis.A person submits a sample and fills the CUNY X-ray Facility Submission form with identification of the researcher, affiliation, chemical information, crystallization solvents and methods, a preliminary chemical structure, optical activity, chemical nomenclature of the compound, molecular numbering system, synthetic schemes, etc. The form also asks if the sample should be returned or destroyed after the X-ray analysis. 2. The sample is examined under the microscope to see if it is suitable for single-crystal X-ray analysis. 3. The sample is either accepted for X-ray analysis or rejected as judged from the microscopic information. Many times it is accepted on a conditional basis. The condition is usually that attempts will be made to collect data but nothing is assured that a crystal from the sample will produce a molecular structure. If a sample is accepted, data is collected and then reduced to obtain structure factors, which are used to solve and refine the molecular structure. The final products of the single-crystal X-ray analysis are ORTEP drawing(s) and a CIF file of the molecular structure, which can be used for publication."
  3. Contact
    00000136-a791-d99f-949b-425080000000
  4. Service Provided by
    X-ray Diffraction Facility
  5. Website(s)
    http://genecenter.hunter.cuny.edu/index.php/facilities/x-ray-diffraction-facility
  6. Related Technique
    Imaging technique
 
RDFRDF
 
Provenance Metadata About This Resource Record
  1. workflow state
    Published
  2. contributor
    sgarner
  3. created
    2012-04-12T12:44:42.117-05:00
  4. creator
    sgarner
  5. modified
    2012-04-12T12:54:19.086-05:00

Copyright © 2016 by the President and Fellows of Harvard College
The eagle-i Consortium is supported by NIH Grant #5U24RR029825-02 / Copyright 2016